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-   -   ATI ICP-OES testing compared to my own testing (http://www.canreef.com/vbulletin/showthread.php?t=126748)

Frogger 08-30-2018 05:56 PM

ATI ICP-OES testing compared to my own testing
 
I just received my first analysis from ATI for my tank water and I did a complete test of my parameters using normal available test kits at the same moment I took the sample and sent it in.

What i have found is I am only really close in 2 parameters salinity and copper. Everything else is off and some by quite a bit.

Alkalinity I tested 8.4 with hanna and 8.5 with Salifert. The actual number was 8.1.

Calcium- I tested 430 with Salifert, 450 with Salifert Strontium test kit. The actual value was 409.

Phosphate ppm tested using hanna ULR at .043 actual was .01.

Nitrates using Red Sea Pro at 1.2ppm it was .01ppm

Mg tested using salifert ppm at 1500 actual is 1415ppm

K tested at 370ppm Salifert actual is 452.

Strontium tested at <3ppm with Salifert actual is 7.8ppm.

So based on my testing I was running GFO to lower phosphates and worried about my Magnesium being too high and my Strontium being too low. In the end ATI is recommending that I stop GFO add phosphate, iodine, molybedenum, Vandium, manganese and Floride everything else looks good. I also need to change my DI resin. Silicates are a little high

How do I trust my personal readings and make appropriate changes when the numbers are not even close? I have no reason to doubt ATI's numbers

And by the way copper was only close because both tested none. I believe the Salifert cu test kit is only really designed when treating parasites in a quarantine system. So that was a no brainer.

I chose ATI because from what I read and saw they appeared to be the best and they also test RO water as well.

WarDog 08-30-2018 07:11 PM

Sending a sample in for testing is just the latest money making fad in our hobby IMPO. Once you get your results back you just end up 'chasing the numbers'.

Just my 2 cents.

Frogger 08-30-2018 07:52 PM

Quote:

Originally Posted by WarDog (Post 1029869)
Sending a sample in for testing is just the latest money making fad in our hobby IMPO. Once you get your results back you just end up 'chasing the numbers'.

Just my 2 cents.

Actually it is a lot more than 2 cents. I never used to do testing and would prefer not to.
Unfortunately in my large tank 75 gallon (set up for 3 years) alkalinity, calcium, phosphate and nitrates are incredibly variable and change quickly. When they change quickly my sps go into stress real fast. I have to test alkalinity and phosphate daily. Today my alkalinity could be 7.5 and tomorrow it could be 9.0.

I have to add nitrates to both balance the phosphates in the tank and to keep the corals from loosing colour. I have to monitor these numbers to keep things balanced.

I just want to make sure that what I am testing is actually what it really is.

I have a 35 gallon reef tank that has corals in it (LPS, SPS and zoas), has been set up for 15 years and now never has issues. I only test alkalinity and calcium once a month to make sure the amount of 2 part I add is correct. I rarely do water changes and the corals are doing great. I take out (sell) about 2 pounds of frogspawn a month from this tank. I test for nitrates and phosphates about once every 6 months and it is always exactly the same. .02 phosphates and 2.0 nitrates.

Every tank is different, this hobby is not a 1 system works for all and my tanks are the perfect example. Not really doing anything different in my tanks, feed the same equal number of corals and fish inch per gallon, same corals.

WarDog 08-30-2018 08:19 PM

I have so much to say but so little time. Let's discuss at Macna.

Frogger 08-30-2018 09:18 PM

Quote:

Originally Posted by WarDog (Post 1029875)
I have so much to say but so little time. Let's discuss at Macna.

Like I said its a lot more than 2 cents.

gregzz4 08-31-2018 12:45 AM

Glen, are you running dosers on your 75g?
Mine never fluctuates like yours, but I don't bother to test daily. I test weekly and adjust my timers accordingly and this keeps things stable.

Frogger 08-31-2018 03:16 AM

Quote:

Originally Posted by gregzz4 (Post 1029885)
Glen, are you running dosers on your 75g?
Mine never fluctuates like yours, but I don't bother to test daily. I test weekly and adjust my timers accordingly and this keeps things stable.

I have a Kamoer doser but I haven't set it up. Currently I am dripping (Tunze auto top off) kalkwasser and supplementing with 2 part when necessary. My house is quite dry (air conditioner) and I lose a lot of water a day to evaporation and I can almost keep my levels correct with the kalkwasser.

gregzz4 08-31-2018 03:24 AM

Hmm. I'd get away from adding kalkwasser in conjunction with your ato, and I'd probably stop the kalk altogether. You don't need it. I've never used it.
It's too aggressive and hard on pumps.
This may be why your alk is swinging, because it's tied into your ato, which is not consistent.

Separate your ato from everything, remove the kalk, and start testing daily for Alk and Ca. Then you'll see some stabiblity and can move forward with your 2-part additives.
I bet you see stability and your dosing will balance out.

Then set up your doser and you'll be much happier with weekly testing.

gregzz4 08-31-2018 03:29 AM

Oh, and don't worry about the results you got back from ATI.
As long as you're close to the proper results with your kits, as I see you were, it's not worth worrying about. Your kits are doing just fine.

I think your Kalk addition is what's stressing out your corals as your ATO will fluctuate, so then will your Alk.

Frogger 08-31-2018 05:16 AM

Quote:

Originally Posted by gregzz4 (Post 1029896)
This may be why your alk is swinging, because it's tied into your ato, which is not consistent.

Only started adding Kalk in the past couple months or so because my phosphates and nitrates shot through the roof when my large yellow tang died and I couldn't find the body. I have been having stability issues for well over a year and a half basically since I started dosing nitrates.

I added the Kalk to help stabilize the phosphate. I didn't want to have to get too aggressive with the GFO.

I have added Kalk before without too much problem.


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